Safe system operation
In addition to familiarization with the correct handling procedures of cryogenic fluids, safe system operation in a cooled sealed system requires some form of positive-pressure safety valve. The safety valve is necessary to avoid the hazard created by a rapidly expanding volume of gas in a closed container. A leak in the system above the coolant level would allow moisture-laden air to be drawn in and possibly freeze the leak closed. As the defective system is then withdrawn from its dewar, the entrapped gas expands rapidly and the excess pressure within in turn causes the gas to expand even more violently. If the leak occurs below the coolant level, the gas generated by the cryogenic fluid trapped upon withdrawal will increase the internal pressure. The accompanying gas-to-liquid volume-ratio table gives the approximate gas-to-liquid volume ratio to be expected at standard temperature and pressure of liquid nitrogen, liquid air, and liquid helium.
In practice, a rubber stopper or plug (Fig. 7) provides a basic safety valve. Prior to evacuating the system, the plug is placed in position over the opening provided. A somewhat more complicated scheme must be employed if a heat-exchange gas is to be used within the system. In either case, the system must be completely checked for leaks prior to cooling to ensure system integrity and safety to personnel.
[1] The heat exchange gas must remain gas at the anticipated cooled temperature of operation. For example, dry helium gas would be used in a nitrogen-cooled system. However, nitrogen gas might liquefy in a helium-cooled system.
[2] For example, a 1-kΩ, ¼-W carbon resistance increases to ≈ 32 kΩ when immersed in liquid helium.